dc.contributor.author |
Kitson, TM |
|
dc.contributor.author |
Loomes, KM |
|
dc.coverage.spatial |
United States |
|
dc.date.accessioned |
2022-06-13T03:06:49Z |
|
dc.date.available |
2022-06-13T03:06:49Z |
|
dc.date.issued |
1985-05 |
|
dc.identifier.citation |
(1985). Analytical Biochemistry, 146(2), 429-430. |
|
dc.identifier.issn |
0003-2697 |
|
dc.identifier.uri |
https://hdl.handle.net/2292/59778 |
|
dc.description.abstract |
In 1982, methyl 2-pyridyl disulfide was reported as a new reagent for the titration of thiol groups in peptides and proteins and for their temporary blocking with the thiomethyl group [T. Kimura et al. (1982) Anal. Biochem. 122, 274-282]. We have synthesized this compound (and its 4-pyridyl isomer) by a rapid and convenient procedure which is preferable to that in the original report. Our method involves the thiomethylation of the appropriate thiopyridone by methyl methanethiosulfonate. |
|
dc.format.medium |
Print |
|
dc.language |
eng |
|
dc.publisher |
Elsevier BV |
|
dc.relation.ispartofseries |
Analytical biochemistry |
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dc.rights |
Items in ResearchSpace are protected by copyright, with all rights reserved, unless otherwise indicated. Previously published items are made available in accordance with the copyright policy of the publisher. |
|
dc.rights.uri |
https://researchspace.auckland.ac.nz/docs/uoa-docs/rights.htm |
|
dc.subject |
Methyl Methanesulfonate |
|
dc.subject |
Sulfhydryl Compounds |
|
dc.subject |
Pyridines |
|
dc.subject |
Sulfhydryl Reagents |
|
dc.subject |
Chemistry |
|
dc.subject |
Chemical Phenomena |
|
dc.subject |
0601 Biochemistry and Cell Biology |
|
dc.subject |
0301 Analytical Chemistry |
|
dc.subject |
0399 Other Chemical Sciences |
|
dc.title |
Synthesis of methyl 2- and 4-pyridyl disulfide from 2- and 4-thiopyridone and methyl methanethiosulfonate. |
|
dc.type |
Journal Article |
|
dc.identifier.doi |
10.1016/0003-2697(85)90563-9 |
|
pubs.issue |
2 |
|
pubs.begin-page |
429 |
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pubs.volume |
146 |
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dc.date.updated |
2022-05-03T05:12:45Z |
|
dc.rights.holder |
Copyright: The author |
en |
dc.identifier.pmid |
4025805 (pubmed) |
|
pubs.author-url |
https://www.ncbi.nlm.nih.gov/pubmed/4025805 |
|
pubs.end-page |
430 |
|
pubs.publication-status |
Published |
|
dc.rights.accessrights |
http://purl.org/eprint/accessRights/RestrictedAccess |
en |
pubs.subtype |
Journal Article |
|
pubs.elements-id |
126966 |
|
pubs.org-id |
Science |
|
pubs.org-id |
Biological Sciences |
|
pubs.org-id |
Science Research |
|
pubs.org-id |
Maurice Wilkins Centre (2010-2014) |
|
dc.identifier.eissn |
1096-0309 |
|
dc.identifier.pii |
0003-2697(85)90563-9 |
|
pubs.record-created-at-source-date |
2022-05-03 |
|