Abstract:
The general part of the experimental section [1] has been presented elsewhere. nBuLi (1.6 M) (6.8 mL, 10.8 mmol) was added to a solution of propargyl alcohol 1 (0.35 mL, 4.9 mmol) in THF (10 mL) under nitrogen at 20°C and the mixture stirred for 10 min. ...