Kinetic Resolution in the Asymmetric Dihydroxylation of 1,7-Dioxaspiro[5.5]undec-4-enes,

Kinetic Resolution in the Asymmetric Dihydroxylation of 1,7-Dioxaspiro[5.5]undec-4-enes,

Brimble, Margaret ; Johnston, Andrew
Identifier: http://hdl.handle.net/2292/8102
Issue Date: 1997
Reference: TETRAHEDRON-ASYMMETR 8(10):1661-1676 22 May 1997
Rights: Copyright: 1997 Elsevier Ltd.
Rights (URI): https://researchspace.auckland.ac.nz/docs/uoa-docs/rights.htm

Abstract:

The asymmetric dihydroxylation of unsaturated spiroacetals 1, 2, 3 was effected using the cinchona alkaloid ligands (DHQ)2-PHAL. (DHQD)2-PHAL and DHQ-IND, DHQD-IND with OSO4, K3Fe(CN)6 and methanesulfonamide. Kinetic resolution of the spiroacetals was achieved and the reactions were monitored by chiral gas chromatography.

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DOI: 10.1016/S0957-4166(97)00152-3
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